RITTER MilliGascounter
– klein, fein und so präzise!

MilliGascounter

Die patentierten MilliGascounter (MGC) eignen sich zur Messung kleinster Gasvolumina bei geringsten Volumenströmen. Sie sind zur Messung aller inerten, schwach aggressiven Gase wie z.B. Biogas und aggressiven Gase sowie für eine volumetrische Leckraten-Messung geeignet.

Table of Contents

Features

  • Minimum flow rate 1 ml/h
  • Maximum flow rate 1 ltr/h
  • Resolution 3 ml
  • Accuracy ± 3 % of reading across full flow rate range; in combination with »RIGAMO« software better than ±1 %
  • Use with inert and medium corrosive gases (biogas) as well as highly aggressive gases
  • Materials: Plexiglas (PMMA), PVDF, PVC (red)
  • Digital counter with programmed calibration factor
  • Battery operated; battery life-time 3-4 years
  • Low-maintenance

Advantages

  • Individual volumetric calibration of each MilliGascounter traceable to the German National Primary Standard (PTB)
  • Total gas production measured (instead of Methane only)
  • Head space volume of fermentation bottle at measurement start (= air) not erroneously measured as pure methane volume

Application

RITTER MilliGascounters (1) (MGC) are designed for the volumetric measurement of the smallest amounts of gas with ultra-low flow rates. They are suitable for measurement of all inert, slightly corrosive gases such as biogas (PMMA model) and aggressive gases (PVDF model). Furthermore, MilliGascounters can be used for volumetric leak detection. (1) Developed at the University of Applied Sciences Hamburg, Prof. Dr. Paul A. Scherer

Inside RITTER MilliGascounter Production (Video EN)

Measurement Principle with Schematic

The gas to be measured flows in via the gas inlet nozzle (3), through the micro capillary tube (9) located at the base of the MilliGascounter and up into the liquid casing which is filled with a packing liquid (12). The gas rises as small gas bubbles through the packing liquid, up and into the measurement cell (13). The meas- urement cell consists of two measuring chambers, which are filled alternatingly by the rising gas bubbles. When a measuring chamber is filled, the buoy- ancy of the filled chamber causes the measurement cell to abruptly tip over into such a position that the second measuring chamber begins to fill and the first empties. The measurement of gas volume therefore occurs in discrete steps by counting the tilts of the measurement cell (13) with a resolution of approximately 3 ml (= content of one meas- uring chamber, please refer to par. 3.2. below). This “residual error” (= max. 3 ml) caused by the resolution should be taken into account when estimating/calculating the total meas- urement error. The tilting procedure of the measurement cell creates by the permanent magnet (11) on top of the cell and one of the two magnetic sensors (reed contacts) (10) a pulse which is registered by the counter unit (1). For external data logging (PC) the switching pulses of the second reed contact can be obtained via the signal output socket (2). (Please refer to par. 4.3 “Signal Output”). The measured gas exits through the gas outlet nozzle (4).
Schematische Darstellung RITTER MilliGascounter (Vorderansicht)
Schematische Darstellung RITTER MilliGascounter (3 Ansichten)

Legend

  1. Counter unit with LCD display
  2. Signal output socket (reed contact)
  3. Gas inlet
  4. Gas outlet
  5. Screw plug for filling
  6. Gas inlet channel
  7. Casing
  8. Base plate
  9. Micro capillary tube
  10. Two reed contacts
  11. Permanent magnet
  12. Packing liquid
  13. Measurement cell (tilting body) with twin-chambers
  14. Tracing screw for liquid level (with MilliGascounter MGC-1 PMMA)
  15. Inspection screw gas inlet channel

Measuring-Range

The minimum flow rate is theoretically zero ltr/h as there are no mechanical limitations with the MilliGascounter which would define a minimum flow. However, at such micro flow rates there are external influences becoming evident: temperature and pressure variation, tightness of the tube connection, permeability of the gas inlet hose. Therefore, the minimum flow rate was defined as 1 ml/h. The maximum flow rate is 1.0 ltr/h.

Accuracy

Because of the physical measurement principle, the measurement error is dependent on the flow rate and it rates ±3 % across the full flow rate range. Each MGC is individually calibrated at the standard flow rate of 0.5 ltr/h so that the measurement error is approx. 0% at this flow rate. At minimum flow rate the measurement error is approximately +3 %, at maximum flow rate approximately -3 %. The »RIGAMO« software (available as accessory) provides an algorithm which automatically recalculates the actual measurement data into the real volume at the respective actual flow rate on the basis of the calibration curve. The remaining error is smaller than ±1% across the full flow rate range.

Performance Data

Minimum flow Qmin 1 ml
Maximum flow Qmax 1 ltr/h
Measurement accuracy (1) ±3 | ±1 %
Measuring drum volume, approx (2) 3 ml
Min. measuring volume (resolution) (3) 3 ml
Packing liquid quantity, approx 120 ml
Diameter 98 mm
Height 109 mm
Weight 475 to 650 g
Maximum gas inlet pressure 100 mbar
Minimum gas inlet pressure 8 mbar
Gas inlet pressure at start of measurement (5) 9 mbar
Gas Temperature (4) 10 to 60 / 80 / 40 °C
Minimum dial division (6) 0,01 ml
Maximum indication value (6) 999.999,99 ml
Connection gas in/outlet Schlauchverschraubung
Outside-Ø 6 mm
Inside-Ø 4 mm
  • (1) Because of the physical measurement principle, the measurement error is dependent on the flow rate. The data acquisition software »RIGAMO« (accessory) provides an algorithm, which automatically recalculates the actual measurement data to the real values at the respective actual flow rate on the basis of the calibration curve. Thus, the remaining error can be reduced significantly or the flow rate range can be extended at the constant measurement error of ±3%. The remaining error is better than approx. ±1% across the full flow rate range.
  • (2) = Nominal value; exact value will be determined by individual calibration
  • (3) = Volume of measuring chamber
  • (4) Max. Operating temperature for PMMA/PVDF/PVC. For complete MGC unit applies: With temperatures > room temperature (e.g. if placed in heating furnace) a foam formation of the packing liquid was monitored in particular cases.
  • (5) The minimum gas inlet may be increased if the measurement starts with a high flow rate. In this case a higher pressure is needed until the micro capillary in the base plate is clear of packing liquid.
  • (6) Because of calibration factor with 2 decimals

Display, Signal Output

The volume of the measured gas is displayed on the electronic digital display located on top of the MGC casing. Additionally a floating reed contact can be used as a signal output.

Data Acquisition with PC

For data acquisition of gas volume and flow rate the Windows software »RIGAMO« is available. The data of up to 24 Ritter gas meters can be transmitted to the USB port of a PC.

Available Models (Materials)

The MGCs are available in the following casing/measurement cell materials:
  • PMMA/PVDF
  • PVDF/PVDF
  • PVC-red/PVC-red

Standard Equipment

  • Zwillings-Messkammer
  • LCD-Anzeige, rückstellbar, 8-stellig
  • Impulsgeber V6.0 (Reed-Kontakt), als Signalausgang (potentialfrei)
  • Libelle
  • Anschlussschlauch (PVC), 1,5 m
  • Schlauchverschraubung für Anschlussschlauch:
  • Gas-Eingangs/Ausgangs-Stutzen:
  • Befüllungs-Trichter
  • Sperrflüssigkeit, 200 ml
  • Spritze, (zur Absaugung von Sperrflüssigkeit)
  • Reinigungsstift für Mikrokapillare, für je 1 bis 5 Stück MilliGascounter

Accessories

  • HCl-Lösung 1,8 Vol% für Gasgemische mit CO2
  • Erhältliche Mengen: 100 / 200 / 500 / 1.000 / 5.000 ml
  • Sperrflüssigkeit Silox Sperrflüssigkeit für Gasgemische ohne CO2
  • Filter 0,45 mikron für Gaseingangsschlauch
  • Filter-Rückschlagventil-Kombination
  • Rückschlagventil für Gaseingangsschlauch

Data-sheets

Downloads

Schlagwörter